NANOGRAPHY - SAXS - WAXS - GISAXS
NANOSTAR unparalleled modular characteristics, it is through a small Angle X-ray scattering (SAXS), swept into the small Angle X-ray scattering (GI - SAXS), wide Angle X-ray scattering (WAXS) and Nanography, for characterizing the structure and nano structure on the surface of the ideal tool.Support mirror adjustment of pinhole collimation system provides a high strength and low parasitic scattering parallel wiring harness, and keep the ideal circular beam shape.Large (XL) sample room can accommodate a variety of special sample stage and the third party sample table, under any condition, so that you measured on various types of samples.Finally, you will be able to pass big background, highly sensitive, low 2 d detector, collect samples of isotropic and anisotropic scattering signal.
This unique X-ray source without water, can provide very stable high strength point focusing X-ray beam.Thanks to its rugged design, the gamma ray source with 3 years warranty.I (including S contains MONTEL integration, advanced 2 d beam plastic optical device, can achieve the highest intensity on the sample.The multilayer reflector design side by side can capture gamma ray source sent out large solid Angle x rays, and effectively in the highly parallel monochromatic beam redirect.
This very convenient very large (XL) sample room added many hole, can run under the condition of vacuum, inert gas or air.It can accommodate many other standard components, easy for you to multiple samples, the third party and the personalized customization stage, for maximum visibility.And electric with large moving range of x-y table and auxiliary electric reference samples wheel, can let you more easily to automatic alignment as well as the reference sample and background scanning!
Using MikrogapTMTechnology VANTEC - 500-2 - D detector can be ideal to meet all the requirements of special SAXS system.First of all, no gas, water or routine maintenance, you also need not worry about radiation damage or movement, therefore, the probe is very strong and easy to use.Large effective area (14 cm in diameter), which can realize large Angle coverage, at the same time bring full field of vision.Very low background and high count rate, the biggest can achieve good dynamic range, and is very sensitive to the sample of weak scattering.Good spatial resolution, can solve the problem of small spacing scattering.At present, there is no other detector can provide this kind of ideal for the application of the function of the combination.
I (including micro JiaoYuan S
MONTEL mirror
SCATEX pinhole
The advanced sample
VANTEC - 5002 - d detector
Small Angle X-ray scattering (SAXS) is embedded into the phenomenon caused by different electron density of particles in the matrix.If particle size between 1 nm - 200 nm, the scattering Angle in the range of 0 ° to 5 °, depending on the use of X-ray wavelength.The smaller the particle, the greater the scattering Angle.
In any medium, any particle arrangement shows the difference of electron density, in the SAXS experiments, this results in a specific pattern.In addition to the particle size, SAXS can also identify the shape, distance and particle size distribution of 2 d graphics.Particles can be dissolved macromolecule, metal precipitation, biological tissue of mineral particles and surfactant micelle.
Compared with the SAXS, wide Angle X-ray scattering (WAXS) identification is the Angstrom level structure, is usually a crystal structure of planar spacing.WAXS is typically used for analysis of Prague, X-ray diffraction (XRD), which helps confirm crystal structure, crystallinity, crystallite size and phase composition (ID).Just put the second detectors in a more close to the location of the sample, can be in WAXS data collected at the same time, obtain SAXS data.
For detection of surface and subsurface structure details, we will with grazing incidence geometry measurement of the sample.Incident Angle is close to the so-called total reflection critical Angle, usually between 0.1 ° and 0.7 °.In swept into the small Angle X-ray scattering (GISAXS) experiment, we can through the 2 d detector, collect scattered in non coplanar direction of scattering intensity data.
With special electric tilt function of GI - SAXS sample machine is mainly used to aim the sample beam.
In Nanography study, using the integration in the NANOSTAR electric machine x-y sample in sample room.Therefore, you can through the X-ray beam to automatically scan samples of the selected area.Then, can through the outline color code, to show the strength distribution of the scattering parameters (or other) information.
Nanography test non-uniform samples quickly and selectively related measurement point, can even pinpoint smaller samples.Complete Nanography said every measurement point of 2 d image collected SAXS/WAXS integral strength.
SAXS: PVDF
Nanography: wood
SAXS: samples of micelle
SAXS: collagen fibers
GI - SAXS
SAXS: LCD
function | parameter | advantage |
I (including micro JiaoYuan S | Air cooling, high strength, microfocus X-ray source |
Low power consumption (30 w) Standard 3 years warranty No cold water machine High power density will increase strength Integrated Montel mirror which can realize the ideal beam adjustment |
SCATEX pinhole |
The ideal circular beam shape, parasitic background scattering is negligible. |
No parasitic aperture edge scattering High resolution/higher flux Detector collimating beam path is more compact, distance is longer Stable pinhole on easily |
XL sample room |
Large sample room with electric samples of x-y table, used in general, standards, and the third party sample localization, mapping, and accommodate the sample machine. |
Internal size: 287 mm x 501 mm x 380 mm (width x height x deep) Use flange connection other power supply Samples of x-y table, translation 80 mm X 130 mm Electric reference sample wheel Can operate in a vacuum, air or inert gas |
VANTEC - 5002 - d detector |
Active area is big, low background, high sensitivity of 2 d detector |
Large effective area (14 cm cm in diameter), is used to view all the SAXS/WAXS scattering image Very low background, therefore, is very sensitive Better spatial resolution pixels (68 microns) Free maintenance (without water/air, or to the main beam or moving sensitive detectors under bias) |
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