X-ray diffraction (XRD)

The D8 ADVANCE Plus

Let the D8 ADVANCE beyond powder were analyzed

Bright spot

The D8 ADVANCE Plus: multi-purpose materials research

> 1 x10 antispasmodics photons per second
EIGER2 R 500 k count rate
EIGER2 R 500 k have the greatest dynamic range, can be realized without absorption measurement and signal-to-noise ratio.
3 x 2
TWIN and for any partial or optical devices
Can be as high as 6 kinds of automatic switching between different beam geometry.
4
Central axis
Compact euler ring plus by adding Phi and Psi, the D8 ADVANCE from 2 axis diffraction into four axis diffractometer.
Brooke exclusive collimating guarantee
For more information

D8 ADVANCE Plus: has the maximum flexibility, to bring you an unprecedented ease of use

D8 ADVANCE Plus is D8 ADVANCE another version, is a multi-purpose, multi-user laboratory platform for the ultimate version of X ray.It is ideal to meet your demand for all types of sample, including powder, block material, fiber, sheet and film (amorphous, polycrystalline and extension) :

  • Typical X-ray powder diffraction (XRD)
  • Analyzing the distribution function (PDF)
  • Small Angle X-ray scattering (SAXS) and wide Angle X-ray scattering (WAXS)
  • X-ray reflectivity (XRR) and high resolution XRD (rocking curve, reciprocal space scanning) environmental conditions and environmental conditions

One of the advantages of this system is that it can be in as many as six different switching between beam geometry: focus from Brentano used for powder Bragg geometry for epitaxial film of high resolution parallel beam of alpha 1 K geometry as well as the switching between the two.You just need to press the button, the software is in our hands.

No matter you are using the sample of the types and want what applications, whether you are a novice user or expert users, are suitable for this: the D8 ADVANCE Plus has unmatched flexibility and ease of use, in terms of data quality, set a new benchmark.

The characteristics of

The main features

The D8 ADVANCE Plus the main function

For any partial or light path

Patented for any partial or the operation of the light path, simplifies the D8 ADVANCE, make it suitable for a variety of applications and sample types.For convenience of users, the system provides the function of automatic electric switch, can be in as many as six different automatically switch between beam geometry.Without human intervention, system in three light path switching between:

  • Used for the analysis of the powder Bragg - Brentano focusing geometry
  • Used in capillary, GID and XRR high strength parallel beam of alpha 1 K, 2 geometry
  • Used for high resolution parallel beam epitaxial film alpha 1 K geometry

It is very suitable for the environmental conditions or environmental condition to analyze samples of all types, including powder, block material, fiber, sheet and film (amorphous, polycrystalline and extension).

The D8 ADVANCE Plus the main function

Materials research samples

Compact ucm and compact euler ring to move the sample machine plus the samples to be able to accurately, thus expanded the D8 ADVANCE plus sample processing capacity.Compact ucm samples可对2Kg的样品进行电动移动:X轴25mm、Y轴70mm和Z轴52mm,可用于分析大型块状样品或多个小样品;紧凑型尤拉环plus样品台的Phi旋转角度不受限制,Psi倾斜度在-5°到95°之间,可用于应力、织构和外延薄膜分析。另外,它还具有真空多用途通孔,可通过小型薄膜样品架或大型手动X-Y样品台,将样品固定在适当位置。二者均可用于温控样品台,进行非环境分析。另外,它们还可借助DIFFRAC.DAVINCI样品台卡口安装系统,轻松更换样品台。

The D8 ADVANCE Plus features

EIGER2 R detector

EIGER2 R with multimodal functions (0 d d - 1-2 d, snapshot and scanning mode), covered from powder research materials from a variety of measurement methods.EIGER2 is not in the traditional sense of the tiger balm, but all the experts in the field of analytical applications.It can be realized without absorption measurement dynamic range, is used for super fast powder and reciprocal space quickly scan the 1 d large size and more than 500 k pixel of 2 d large coverage, and the multiple pattern detector set a new standard.EIGER2 adopted DECTRIS company research and development of beam detector technology, integration of the software and hardware of the brook, will eventually bring you seamless and easy solution.

application

A diffraction - all applications

The D8 ADVANCE Plus the main function

Powder diffraction

X-ray powder diffraction (XRPD) technology is one of the most important material characterization tool.Powder diffraction figure a lot of information, directly from the phase arrangement of atoms.In the D8 ADVANCE and DIFFRAC SUITE software support, you will be able to implement common simply XRPD method:

  • Identify the crystal phase and amorphous phase, and the determination of purity of samples
  • For multiphase mixture of crystal phase and amorphous phase quantitative analysis
  • Microstructure analysis (crystallite size, micro strain, disorderly...).
  • Heat treatment or processing and manufacturing components of a large number of residual stress
  • Texture analysis (preferred orientation)
  • Index, from the crystal structure and crystal structure refinement
The D8 ADVANCE Plus the main function

Residual stress and texture analysis

For industrial metal samples need to explore the material limit, often need, the measurement of residual stress and texture.By eliminating the tensile stress or cause stress on the surface of the sample, can significantly extend the life of its function.This is achieved by heat treatment or physical process to complete the shot blast, etc.Constitute a block sample crystallite orientation, determines the way of crack growth.And through the material formed in the specific texture, can significantly enhance its characteristics.These two technologies in the optimization of sophisticated manufacturing method (for example, to add material manufacturing) field also has its place.

The D8 ADVANCE Plus the main function

Thin film and coating

Thin film and coating analysis using the principle of the same as the XRPD, but further provides the Angle of beam adjustment and control function.Typical examples include, but are not limited to phase identification, crystal quality, residual stress, texture, thickness and composition and the strain analysis.The analysis of thin film and coating, of thickness between the nm and including m analyses characteristics of layered materials (from amorphous and polycrystalline coatings to epitaxial film).The D8 ADVANCE and DIFFRAC SUITE software high-quality film can make the following analysis:

  • Grazing incidence diffraction
  • X-ray reflection method
  • High resolution X ray diffraction
  • Reciprocal space scanning

Technical parameters

The D8 ADVANCE Plus specifications

function

specifications

advantage

For any partial or light path

Software switch button:

Motor drive divergence slit geometry (BB)

High strength Ka1, two parallel beam

High resolution Ka1 parallel beam

Patents: US10429326, US6665372, US7983389

Can be in as many as six different automatic electric switch between beam geometry, without human intervention

Is ideal for all types of sample analysis, including powder, block material, fiber, sheet and film (amorphous, polycrystalline and extension)

LYNXEYE XE - T

Energy resolution: < 380 eV @ 8 KeV

Test mode: 0 d, 1 d and 2 d

Wavelength: Cr, Co, Cu, Mo and Ag

Patents: EP1647840, EP1510811, US20200033275

To decide without K with filter and secondary monochromator

Iron radiation can be 100% filter fluorescence

450 times faster than conventional detector system

BRAGG 2 d pattern: use the divergence of the primary data collected 2 d wiring harness

Unique detector guarantee: when delivery is not bad

EIGER2 R

EIGER2 R

Dectris company development based on hybrid photon counting technology of a new generation of detectors, support for multiple model (0 d / 1 d / 2 d)

In continuous scanning step scanning, and seamless integration in the advanced scanning mode 0 d, 1 d and 2 d test

Ergonomic from probe rotating function, can optimize the gamma or 2 Ɵ Angle range

Use full detector, free tools panoramic view of the diffraction beam optical systems

Continuous variable detector position to balance the Angle range and resolution

Rotating light tube

Online focal spot and point between focal spot applications quickly and easily for free on the switch

Don't need to disconnect cables or pipes, without having to remove the pipe

DAVINCI design: the automatic detection and configuration focusing direction

Compact ucm samples

X axis mobile range: 25 mm

Y mobile range: 70 mm

Z axis mobile range: 52 mm

Load weight: 2 kg

Accurate positioning the beam medium the interested area of the sample

Support multiple sample installation, for automatic measurement

Compact euler ring Plus samples

Motor drive Phi axis: is not restricted

Motor drive Psi axis: - 5 ° to 95 °

The vacuum multifunctional hole, easy to install sample

All four axis diffraction, support texture, residual stress and thin film measurements

The D8 goniometer

With independent double circle of step motor and optical encoder goniometer

Brooke unique collimating guarantee, ensure the accuracy and precision of unparalleled

Absolutely free maintenance drive/gear, lubrication for life

Absolutely free maintenance drive/gear, lubrication for life

The environmental conditions

Temperature: from 4 k to 2500 k

Pressure: 10 - ⁴ mbar to 100 bar

Humidity: 5% to 95%

In the environment and the environmental conditions were studied

The DIFFRAC designed to help you easily replace the sample units

accessories

XRD components

XRD components

Bruker XRD solution contains a series of high-performance components to meet the demand of analysis.Modular design is the key to make the best instrument.

All kinds of components are brooke component part of the core competitiveness, they are made from brooke AXS development or, or by close cooperation with the third party suppliers.

Brooke XRD components can be used to upgrade the existing X-ray system, is used to improve its performance.

software

Use the DIFFRAC. SUITE planning, measurement and analysis

Dave's SUITE software

DIFFRAC. SUITE ™ brought rich software modules, allowing you to easily implement X-ray powder diffraction data collection and evaluation.Based on the Microsoft.net technology, DIFFRAC. Offers all the advantages of the technology of modern software SUITE, in order to realize the stability, the greatest of ease of use and connected to the Internet.

Fully customizable user interface is the feature of plug-in framework, provides a general appearance, feelings and actions.All the measurement and evaluation software module can run as a standalone application, also can be integrated to DIFFRAC. The SUITE of plug-in framework.Unlimited Internet access and control allows customers to network within any number of D2 PHASER, D8 ADVANCE, D8 DISCOVER and D8 ENDEAVOR diffractometer.

Measuring software:

WIZARD - method of planning

COMMANDER - method and direct measurement

TOOLS - instrument control tool entry:

Powder diffraction software:

DQUANT - quantitative analysis

EVA - phase identification and quantitative analysis

TOPAS - peak type analysis, quantitative analysis and structure analysis

Materials research software:

SAXS - small Angle X ray scattering software

XRR, comprehensive analysis of the X-ray reflection

TEXTURE - full of TEXTURE analysis meet the ease of use

Residual stresses LEPTOS - film analysis/research

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support

Service and support

We offer:

  • Professional senior technical personnel to do fault professional technical support, isolation and solve the problem of hardware and software
  • Network remote service, providing diagnosis and application support
  • Fusion reality support - virtual engineers in your side,video)
  • According to your request to schedule maintenance
  • Customer site maintenance, maintenance services
  • Spare parts delivery will be within one working day/the world needs a few working days to complete
  • Installation qualification and operational qualification/performance verification of compliance services
  • Site planning and relocation
  • Find nextA training course

Check out ourSupport site:

  • Software updates
  • Product manuals and installation guide
  • Training video

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